KARAKTERISASI DIFRAKSI SINAR X PADA PEMBUATAN FILM TIPIS BARIUM ZIRKONIUM TITANATE BaZrxTi(1-x)O3 DENGAN MENGGUNAKAN METODE SOL-GEL
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Date
2021-03
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Abstract
Barium Titanate (BaTiO3) is a ferroelectric material that has a high dielectric constant value,
which can be made in the form of a thin layer. A thin layer of Barium Titanate (BaTiO3) doped
with Zr to form Ba (ZrxTi1-x) O3 was successfully prepared using sol gel method with the
composition of x = 0.2 and x = 0.4. A thin layer was created on the glass substrate using a spin
coating for 30 seconds at a speed of 3000rpm. BZT was annealed with temperature variations of
600oC and 650oC and characterized using X-Ray Diffractometer (XRD) to determine lattice
parameters, crystalline structure, and crystalline size using the Scherrer formula. Based on the
analysis, the thin layer has a tetragonal crystalline structure with the lattice parameters value for
the composition x = 0.2 is a = b = 4.02 Å and c = 4.06 Å, the composition x = 0.4 is a = b = 4, 06
Å and c = 4.10Å. The crystal size for x = 0.2;0.4 with a temperature of 600oC and 650oC are
33,84 nm, 45,05 nm, 50,66 nm, dan 67,54 nm respectively.
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Keywords
Barium Zirconium Titanate, Sol Gel Method, Annealing, XRD Characterization